Details
99% Purity Commercial production Citrazinic acid 99-11-6 with Cheapest Price
- Molecular Formula: C6H5NO4
- Molecular Weight: 155.11
- Appearance/Colour: yellow powder
- Vapor Pressure: 3.56E-07mmHg at 25°C
- Melting Point: >300 °C
- Refractive Index: 1.5423 (estimate)
- Boiling Point: 375.5 °C at 760 mmHg
- PKA: 2.54±0.20(Predicted)
- Flash Point: 180.9 °C
- PSA: 90.65000
- Density: 1.708 g/cm3
- LogP: 0.19100
Citrazinic acid(Cas 99-11-6) Usage
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Purification Methods |
The acid is normally a yellow powder with a greenish shade, but is white when ultra pure and turns blue on long standing. It is insoluble in H2O but slightly soluble in hot HCl and soluble in alkali or carbonate solutions. It is purified by precipitation from alkaline solutions with dilute HCl, and dried in a vacuum over P2O5. The ethyl ester has m 232o (evacuated tube) and a pKa of 4.81 in MeOCH2CH2OH [IR: Pitha Coll Czech Chem Comm 28 1408 1963]. [Beilstein 22/7 V 24.] |
InChI:InChI=1/C6H5NO4/c8-4-1-3(6(10)11)2-5(9)7-4/h1-2H,(H,10,11)(H2,7,8,9)/p-1
99-11-6 Relevant articles
Synthesis method of citrazinic acid
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Paragraph 0010; 0012; 0013, (2018/07/06)
The invention belongs to the technical f...
PROCESS FOR PRODUCTION OF 2-HYDROXY-4-SUBSTITUTED PYRIDINES
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Page/Page column 9-10, (2008/06/13)
A process for preparing a 2-hydroxy-4-su...
99-11-6 Process route
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77-92-9,906507-37-7
citric acid
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-
99-11-6
citrazinic acid
| Conditions | Yield |
|---|---|
|
With
urea;
In
water;
at 185 ℃;
for 2h;
Sonication;
High pressure;
|
85.18%
|
|
With
methanol; toluene-4-sulfonic acid;
Erhitzen des Reaktionsgemisches mit wss. NH3 auf 130grad und anschliessenden Erwaermen mit NaOH;
|
-
-
55-22-1
pyridine-4-carboxylic acid
-
-
22282-72-0
2-hydroxyisonicotinic acid
-
-
99-11-6
citrazinic acid
| Conditions | Yield |
|---|---|
|
With
sodium hydroxide;
In
water;
at 27 - 30 ℃;
for 0.5 - 25h;
pH=7.0;
Product distribution / selectivity;
Medium;
fermentation;
|
|
|
With
sodium hydroxide;
In
water;
at 27 - 30 ℃;
for 0.5 - 25h;
pH=7.0 - 8.5;
Product distribution / selectivity;
Medium;
fermentation;
|
|
|
With
sodium hydroxide;
In
water;
at 27 - 30 ℃;
for 0.5 - 25h;
pH=7.0 - 8.5;
Product distribution / selectivity;
Medium;
fermentation;
|
99-11-6 Upstream products
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725679-43-6
citric acid α,α'-diamide
-
130839-31-5
citric acid α-amide
-
597-59-1
citric acid triamide
-
1587-20-8
trimethyl citrate
99-11-6 Downstream products
-
5398-44-7
2,6-dichloropyridine-4-carboxylic acid
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91013-21-7
ethyl 2-ethoxy-6-hydroxyisonicotinate
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98996-85-1
2,6-dihydroxy-isonicotinic acid-(2-methoxy-ethyl ester)
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91642-09-0
2,6-dihydroxy-isonicotinic acid cyclohexyl ester
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