Citrazinic acid

  • Name: Citrazinic acid
  • CAS: 99-11-6
  • Purity: 99%
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Details

99% Purity Commercial production Citrazinic acid 99-11-6 with Cheapest Price

  • Molecular Formula: C6H5NO4
  • Molecular Weight: 155.11
  • Appearance/Colour: yellow powder 
  • Vapor Pressure: 3.56E-07mmHg at 25°C 
  • Melting Point: >300 °C 
  • Refractive Index: 1.5423 (estimate) 
  • Boiling Point: 375.5 °C at 760 mmHg 
  • PKA: 2.54±0.20(Predicted) 
  • Flash Point: 180.9 °C 
  • PSA: 90.65000 
  • Density: 1.708 g/cm3 
  • LogP: 0.19100 

Citrazinic acid(Cas 99-11-6) Usage

Purification Methods

The acid is normally a yellow powder with a greenish shade, but is white when ultra pure and turns blue on long standing. It is insoluble in H2O but slightly soluble in hot HCl and soluble in alkali or carbonate solutions. It is purified by precipitation from alkaline solutions with dilute HCl, and dried in a vacuum over P2O5. The ethyl ester has m 232o (evacuated tube) and a pKa of 4.81 in MeOCH2CH2OH [IR: Pitha Coll Czech Chem Comm 28 1408 1963]. [Beilstein 22/7 V 24.]

InChI:InChI=1/C6H5NO4/c8-4-1-3(6(10)11)2-5(9)7-4/h1-2H,(H,10,11)(H2,7,8,9)/p-1

99-11-6 Relevant articles

Synthesis method of citrazinic acid

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Paragraph 0010; 0012; 0013, (2018/07/06)

The invention belongs to the technical f...

PROCESS FOR PRODUCTION OF 2-HYDROXY-4-SUBSTITUTED PYRIDINES

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Page/Page column 9-10, (2008/06/13)

A process for preparing a 2-hydroxy-4-su...

99-11-6 Process route

citric acid
77-92-9,906507-37-7

citric acid

citrazinic acid
99-11-6

citrazinic acid

Conditions
Conditions Yield
With urea; In water; at 185 ℃; for 2h; Sonication; High pressure;
85.18%
With methanol; toluene-4-sulfonic acid; Erhitzen des Reaktionsgemisches mit wss. NH3 auf 130grad und anschliessenden Erwaermen mit NaOH;
pyridine-4-carboxylic acid
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pyridine-4-carboxylic acid

2-hydroxyisonicotinic acid
22282-72-0

2-hydroxyisonicotinic acid

citrazinic acid
99-11-6

citrazinic acid

Conditions
Conditions Yield
With sodium hydroxide; In water; at 27 - 30 ℃; for 0.5 - 25h; pH=7.0; Product distribution / selectivity; Medium; fermentation;
With sodium hydroxide; In water; at 27 - 30 ℃; for 0.5 - 25h; pH=7.0 - 8.5; Product distribution / selectivity; Medium; fermentation;
With sodium hydroxide; In water; at 27 - 30 ℃; for 0.5 - 25h; pH=7.0 - 8.5; Product distribution / selectivity; Medium; fermentation;

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