TRIPHENYLTIN HYDRIDE

  • Name:TRIPHENYLTIN HYDRIDE
  • CAS:892-20-6
  • Purity:99%
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Factory Sells Best Quality TRIPHENYLTIN HYDRIDE 892-20-6 with USP

  • Molecular Formula:C18H16 Sn
  • Molecular Weight:351.035
  • Melting Point:28 °C(lit.)
     
  • Refractive Index:n20/D 1.632(lit.) 
  • Boiling Point:163-165 °C0.3 mm Hg(lit.)
     
  • Flash Point:>230 °F  
  • PSA：0.00000 
  • Density:1.374 g/mL at 25 °C(lit.)  
  • LogP:1.93510 

TRIPHENYLTIN HYDRIDE(Cas 892-20-6) Usage

InChI:InChI=1/3C6H5.Sn/c3*1-2-4-6-5-3-1;/h3*1-5H;/q;;;+1/rC18H15Sn/c1-4-10-16(11-5-1)19(17-12-6-2-7-13-17)18-14-8-3-9-15-18/h1-15H/q+1

892-20-6 Relevant articles

Organometallic iridium complexes of (Z)-1-Phenyl-2-(4′,4′-dimethyl-2′-oxazolin-2′-yl)-eth-1-en-1-ate: Structural aspects, reactivity and applications in the catalytic dehydrogenation of Alkanes#

Clément, Roxanne,Gossage, Robert A.,Lough, Alan J.,May, Kathleen L.

supporting information, p. 2042 - 2047 (2021/09/16)

The treatment of [IrCl(cod)]2 with (Z)-1...

Novel amino propyl substituted organo tin compounds

Pichler, Johann,Torvisco, Ana,Bottke, Patrick,Wilkening, Martin,Uhlig, Frank

, p. 565 - 573 (2014/06/10)

In this work, a new synthetic pathway yi...

Stereoselective radical tandem cyclohydrostannation of optically active di-unsaturated esters of TADDOL

Gerbino, Dario C.,Koll, Liliana C.,Mandolesi, Sandra D.,Podesta, Julio C.

, p. 660 - 665 (2009/01/30)

This paper reports the results obtained ...

Efficient syntheses of four stable-isotope labeled (1R)-menthyl (1S,2S)-(+)-2-phenylcyclopropanecarboxylates

Keliher, Edmund J.,Burrell, Richard C.,Chobanian, Harry R.,Conkrite, Karina L.,Shukla, Rajesh,Baldwin, John E.

, p. 2777 - 2784 (2008/09/16)

Many carbenoid cyclopropanation reaction...

892-20-6 Process route

triphenyl-vinyl stannane
2117-48-8

triphenyl-vinyl stannane

2,3,4,5-tetraphenylcyclopenta-2,4-dienone
479-33-4

2,3,4,5-tetraphenylcyclopenta-2,4-dienone

tetraphenyltin(IV)
595-90-4

tetraphenyltin(IV)

triphenylstannane
892-20-6

triphenylstannane

triphenyltin bromide
962-89-0

triphenyltin bromide

Conditions
Conditions Yield
With bromobenzene; In further solvent(s); byproducts: tetraphenylbenzene; refluxing in bromobenzene;;
With C6H5Br; In further solvent(s); byproducts: tetraphenylbenzene; refluxing in bromobenzene;;
lithium aluminium tetrahydride
16853-85-3

lithium aluminium tetrahydride

triphenyltin chloride
639-58-7

triphenyltin chloride

triphenylstannane
892-20-6

triphenylstannane

Conditions
Conditions Yield
In diethyl ether; at 0 ℃; for 4h; Glovebox; Schlenk technique; Inert atmosphere;
94%
In diethyl ether; reacting tin compd. with LiAlH4 in ether (as in: H. G. Kuivila, O. F. Beumel, Jr., J. Am. Chem. Soc., 1961, 83, 1246-1250);
84.1%
In diethyl ether; addn. of (C6H5)3SnCl to an ice-cooled suspension of LiAlH4 in waterfree diethyl ether; warming to room temperature; stirring for 3 h; addn. of ice-water; obtaining of the ether layer;;
78%
In diethyl ether; addn. of (C6H5)3SnCl to an ice-cooled suspension of LiAlH4 in waterfree diethyl ether; warming to room temperature; stirring for 3 h; addn. of ice-water; obtaining of the ether layer;;
61%
In diethyl ether; addn. of (C6H5)3SnCl to an ice-cooled suspension of LiAlH4 in waterfree diethyl ether; warming to room temperature; stirring for 3 h; addn. of ice-water; obtaining of the ether layer;;
58%
In diethyl ether; addn. of (C6H5)3SnCl to an ice-cooled suspension of LiAlH4 in waterfree diethyl ether; warming to room temperature; stirring for 3 h; addn. of ice-water; obtaining of the ether layer;;
42%
In diethyl ether; addn. of (C6H5)3SnCl to an ice-cooled suspension of LiAlH4 in waterfree diethyl ether; warming to room temperature; stirring for 3 h; addn. of ice-water; obtaining of the ether layer;;
77-85
In not given; reaction in ethers;;
In not given;
In diethyl ether;

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